The ESEM is back online.
Just letting you know I put the TEM grids back in my office (MM622).
If are in need of TEM grids let me know.
Those are the ones we currently have available:
- Continuum C-film on copper
- Continuum C-film in nickel
- Lacey C-film on copper
- Silicon oxide Film on copper
- Formvar Carbon single
- Formvar supported lacey C-film on copper
- Quantifoil C-film on copper
- Graphene supported Lacey C-film on copper
Erico Freitas
Seminar
Using Machine Vision to Drive Nanoscale Discoveries That Solve Real-World Problems
Jennifer McConnell
Senior Manager of Marketing & Product Management, Protochips
1 p.m. in ChemSci 102, Zoom available.
Lunch and Learn—In situ TEM
Minerals and Materials 607
Session 1 Corrosion: 11:15 a.m.–12 p.m.
Corrosion is a $2.6 trillion dollar problem that accounts for 3.4% of the global GDP, therefore it is well understood that testing and developing better materials to increase the durability of infrastructure such as bridges and ships could save $375-$875 billion annually. To develop resistant materials and corrosion-effective mitigation strategies, a deeper understanding of materials used, and the corrosion processes must first be elucidated.
Using the in-situ TEM systems from Protochips such as the Atmosphere AX (gas cell) and Poseidon AX (liquid cell), researchers can directly observe corrosion processes such as initiation and progression at the nanoscale in real time and under relevant conditions. By introducing corrosive environments while simultaneously monitoring material responses, valuable insights into the kinetics of corrosion reactions can be observed at the nanoscale.
Session 2 Catalysis: 12:15–1 p.m.
To combat climate change and the release of harmful chemicals in the environment, highly efficient catalysts must be developed. Using Atmosphere AX, the in-situ gas cell system from Protochips, researchers can investigate the morphology and atomic structure of catalyst materials, including nanoparticles, nanowires, and other nanostructures to develop more stable and sustainable catalytic systems. Moreover, in-situ TEM allows researchers to perform nanostructure characterization of catalyst-substrate interactions at high spatial resolutions to better understand catalytic processes including formation and evolution of reaction intermediates, surface restructuring, and catalyst deactivation in real time and under relevant catalytic conditions.
Register to attend once per session.
September 13, 2023
I’m pleased to report that the ESEM repairs will be completed today and the instrument is available as soon as tomorrow morning.
September 8, 2023
Unfortunately, the power supply did not fix this issue. I’ve done as much remote troubleshooting as possible. We will have a service technician on campus next week to look into the issue.
If anyone has any urgent samples, please contact me and we can make other arrangements.
September 7, 2023
Just a quick update. It looks like the filament is not the issue. I have been working with SEMTech to diagnose the problem. They are overnighting me a power supply. We are going to replace it tomorrow. I will have an update at that point.
I know many of you are eager to get back on the instrument. I thank you for your patience.
September 6, 2023
The ESEM is down due to an issue with the filament. We are working on this and hope to have the issue resolved by tomorrow.
The upgrades on the ESEM will be extending into next week. If anyone has set up an appointment with us for training I will contact you individually to reschedule those.
Just a reminder, a brief training will be required before you can operate the instrument without supervision.
If you are ever going to need TEM grids while I’m on vacation (Aug 2-30), please take the TEM grids in the glass desiccator at the MM631.
Please, make sure you follow the TEM Grid Instructions.
Regards,
Erico Freitas
The FESEM is available for imaging, but the EDS system is not currently working.
I’ll be out of town August 2-30 and Joshua King is looking after the STEM while I’m gone.
Please, make sure you double check Joshua King’s schedule and invite him when you reserve time at the STEM so he can assist you during the STEM sessions.
STEM training sessions will resume In September.
If you need TEM grids please let Elizabeth Miller knows.
Kind regards,
Erico Freitas
The AFM is available for use.
Dear ACMAL Users,
I hope this email finds you well. I wanted to inform you that I will be out of town from July 20th – July 31st. Erico will also be out of the office for the Microscopy Conference (July 24-28th).
During this period, if you encounter any issues or have any questions, please reach out to the following contacts:
- For X-ray Facility questions, please contact
- Dr. Ed Laitila at 906-369-2041 or email ealaitil@mtu.edu.
- For Electron Optics Facility questions or sample preparation, please contact
- Josh King at 404-808-2803 or email jorking@mtu.edu
- For Scanning Probe Microscopy (AFM) & Surface Analysis (XPS) Facilities questions, please reach out to
- Dr. Timothy Leftwich at tleftwi@mtu.edu.
- For Confocal Imaging Facility questions, please contact
- Dr. Marina Tanasova at 906-487-1163 or email mtanasov@mtu.edu (Confocal, Cell Culture Lab & Flow Cytometer)
- In case of an emergency, call public safety by dialing 911.
These individuals, as experts in their respective areas, will be able to assist you promptly. However, please note that for general inquiries or matters not specific to a particular area, it is best to contact me upon my return.
I have complete confidence in the ACMAL team’s abilities to handle any issues that may arise during my absence. Thank you for your understanding and cooperation. I will be sure to get back to you promptly upon my return on July 31st.
Wishing you all continued success with your research.
Best regards,
Liz